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Beilstein J. Org. Chem. 2013, 9, 2620–2624, doi:10.3762/bjoc.9.296
Graphical Abstract
Scheme 1: Retrosynthesis of I and I'. PG = protecting group; protecting groups may vary independently.
Scheme 2: Reagents and conditions: (a) TBDPSCl, DMAP, imidazole, CH2Cl2, rt, 99%; (b) DIBAL-H, CH2Cl2, −78 °C...
Scheme 3: Reagents and conditions: (a) MeI, t-BuOK,THF, rt, 96%; (b) AD-mix-β, t-BuOH/H2O, 0 °C, 80%; (c) TEM...
Scheme 4: Reagents and conditions: (a) PhCH(OCH3)2, PPTS, CH2Cl2, rt; (b) DIBAL-H, CH2Cl2, 0 °C, 76% in two s...
Scheme 5: Reagents and conditions: (a) TBSOTf, 2,6-lutidine, CH2Cl2, rt, 90%; (b) CSA, MeOH, 0 °C, 59%. TBS = ...
Scheme 6: Reagents and conditions: (a) Dess–Martin periodinane, CH2Cl2, rt, 86%; (b) TBAF, THF, 0 °C, 84%; (c...
Scheme 7: Reagents and conditions: (a) MeI, t-BuOK,THF, rt, 96%; (b) AD-mix-β, t-BuOH/H2O, 0 °C, 82%; (c) TBS...